By Michael B. Smith
The Compendium of natural man made Methods serves as a convenient laptop reference for natural chemists to browse new reactions and adjustments of curiosity, facilitating the hunt for useful workforce changes within the unique literature of natural chemistry. quantity thirteen includes either sensible crew adjustments and carbon-carbon bond forming reactions from the literature within the years 2005-8. It provides examples of released reactions for the instruction of monofunctional compounds.
The Compendium of natural artificial equipment sequence enables the hunt for caliber, chosen useful workforce differences, geared up by way of reacting sensible workforce of beginning fabric and practical team shaped, with complete references to every reaction
Presents examples of released reactions for the practise of monofunctional compounds from the literature of 2005-8
Provides a convenient reference and a precious software to the operating natural chemist, permitting a short money of recognized natural transformations
Stringent standards for inclusion of reactions, together with actual man made application of reactions, reagents on hand or simply ready and dealt with within the laboratory
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Additional resources for Compendium of Organic Synthetic Methods
2007, 48, 2931 . PhCH, h, 72% 0 2 (balloon ) EtOAc, lO h, 0. -i. ;Itoh , A . Synthesis 2006,1757 . f- B u ,CH 3 ZnO, DM F, microwave s 95°C,6 mi n Gupta, M. ; Paul ,S. ; Gupta , R. ; Loupy , A . Tetrahedron Lett. 2005, 46, 495 . SECTION 21: ACID DERIVATIVES FROM AMIDES NO ADDITIONA L EXAMPLE S SECTION 22: ACID DERIVATIVES FROM AMINES PhCH 2 NH 2 DMSO, N a N 0 2 PhCO-i 1H 92 49%HBr,100°C * Naik,R. A . Synth. Commun. 2006, 36,165 . % SECTION 23: ACID DERIVATIVES FROM ESTERS A, o Ph " O esterase fro m Bacillus subtilis (BS2 ) PhC0 2 H 92% Fotakopoulou,I.
CI ,CHO1. - H . - M . J. Am. Chem. Soc. 2006, 128,14808 . R. J . J. Am. Chem. Soc. 2006, 128,16040 . -Y. -L. -J . J. Org. Chem. 2006, 71,833 . E. ;Fu ,J. M. ;Su ,X. E. D . J. Org. Chem. E. ;Fu ,J. J . J. Org. Chem. 2006, 71,1523 . T. ; Mitsumori ,S. ; Albertshofer , K. ; Tanaka ,F. F . J. Org. Chem. 2006, 71, 3822. OH 90% (88 % ee ) PhCHO Et 2 Zn, 0° C, Id ; H 30 + E t Tanaka, T. ; Yasuda , Y. ; Hayashi ,M . J. Org. Chem. 2006, 71, 7091 . - F . H. - J . ; Zhang , Q. -L . Org. Lett. 2006, 8,1479 .
1, TBDMSC 1 0 HP . DC M. 2- ° C, 16 h 2. F 3 CC0 2 H/DCM 5 6 % M n , [CrCl 2 ]. A. S . Tetrahedron Lett. 2007, 48, 4323 . 1% [RuCl 2 (diphosphine)(diamine)],18 h p ^ 99% (90 % ee ) Li, X. ;List ,B . Chem. Commun. 2007,1739 . I hors elive ralcoho l dehydrogenas ef phosphate buffe r p h - 96% Giacomini, D. ;Galletti ,P. ; Quintavalla , A. ; Gucciardo , G. ; Paradisi ,F . Chem. Commun. 2007, 4038. PhCHO» HC0 2 NH 4, TH F, 25° C • PhCH % 2 OH 85 Ni- n anoparticles ,1,5 h Kidwai, M. ; Bansal , V. ; Saxena , A.